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Chemistry

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Also known as: 2-bromo-2-nitro-1,3-propanediol, 52-51-7, 2-bromo-2-nitropropane-1,3-diol, Bronosol, Bronocot, Bronidiol
Molecular Formula
C3H6BrNO4
Molecular Weight
199.99  g/mol
InChI Key
LVDKZNITIUWNER-UHFFFAOYSA-N
FDA UNII
6PU1E16C9W

Bronopol
Bronopol, or 2-Bromo-2-nitro-1,3-propanediol, is an organic compound with wide-spectrum antimicrobial properties. First synthesized in 1897, bronopol was primarily used as a preservative for pharmaceuticals and was registered in the United States in 1984 for use in industrial bactericides, slimicides and preservatives. Bronopol is used as a microbicide or microbiostat in various commercial and industrial applications, including oil field systems, air washer systems, air conditioning or humidifying systems, cooling water systems, papermills, absorbent clays, metal working fluids, printing inks, paints, adhesives and consumer products. Compared to other aliphatic halogen-nitro compounds, bronopol is more stable to hydrolysis in aqueous media under normal conditions. The inhibitory activity against various bacteria, including Pseudomonas aeruginosa, was demonstrated in vitro. The agent is largely available commercially as an antibacterial for a variety of industrial purposes while it is predominantly available for purchase as a pet animal litter antibacterial at the domestic consumer level. Nevertheless, ongoing contemporary re-evaluations of bronopol use in large markets such as Canada now place various compositional and product restrictions on the use of the agent in cosmetic products and in other products where it may not primarily be used in the role of a non-medicinal preservative antimicrobial.
Bronopol is a Standardized Chemical Allergen. The physiologic effect of bronopol is by means of Increased Histamine Release, and Cell-mediated Immunity.
1 2D Structure

Bronopol

2 Identification
2.1 Computed Descriptors
2.1.1 IUPAC Name
2-bromo-2-nitropropane-1,3-diol
2.1.2 InChI
InChI=1S/C3H6BrNO4/c4-3(1-6,2-7)5(8)9/h6-7H,1-2H2
2.1.3 InChI Key
LVDKZNITIUWNER-UHFFFAOYSA-N
2.1.4 Canonical SMILES
C(C(CO)([N+](=O)[O-])Br)O
2.2 Other Identifiers
2.2.1 UNII
6PU1E16C9W
2.3 Synonyms
2.3.1 MeSH Synonyms

1. 2-bromo-2-nitro-1,3-propanediol

2. Bronosol

2.3.2 Depositor-Supplied Synonyms

1. 2-bromo-2-nitro-1,3-propanediol

2. 52-51-7

3. 2-bromo-2-nitropropane-1,3-diol

4. Bronosol

5. Bronocot

6. Bronidiol

7. Bronopolu

8. Bronotak

9. 1,3-propanediol, 2-bromo-2-nitro-

10. Onyxide 500

11. Lexgard Bronopol

12. 2-nitro-2-bromo-1,3-propanediol

13. Bnpd

14. Mfcd00007390

15. Beta-bromo-beta-nitrotrimethyleneglycol

16. Nsc 141021

17. Chebi:31306

18. Nsc-141021

19. 6pu1e16c9w

20. Ncgc00164057-01

21. Bronopolum

22. Dsstox_cid_4652

23. Dsstox_rid_77484

24. Dsstox_gsid_24652

25. Bronopolu [polish]

26. Caswell No. 116a

27. Bioban

28. Bronopolum [inn-latin]

29. Myacide As Plus

30. Myacide Bt

31. Cas-52-51-7

32. Bronopol [inn:ban:jan]

33. Myacide Pharma Bp

34. Canguard 409

35. Bnpk

36. Hsdb 7195

37. Einecs 200-143-0

38. Un3241

39. Epa Pesticide Chemical Code 216400

40. Brn 1705868

41. Unii-6pu1e16c9w

42. Ai3-61639

43. 2-bromo-2-nitropropan-1,3-diol

44. 2-bromo-2-nitro-propane-1,3-diol

45. Bronopol (jan/inn)

46. Bronopol [hsdb]

47. Bronopol [inn]

48. Bronopol [jan]

49. Bronopol [mi]

50. Bronopol [vandf]

51. Bronopol [mart.]

52. Wln: Wnxe1q1q

53. 1, 2-bromo-2-nitro-

54. 2-bromo-2-nitropropane-1,3-diol (bronopol)

55. Bronopol [who-dd]

56. Ec 200-143-0

57. Schembl23260

58. Bioban Bnpd-40 (salt/mix)

59. Chembl1408862

60. Dtxsid8024652

61. Schembl16556987

62. Lvdkznitiuwner-uhfffaoysa-

63. 2-bromo-2nitro-1,3-propanediol

64. Amy8948

65. 2-bromo-2-nitro-1,3-propandiol

66. 2-bromo-2-nitropropane-1,3-diol [un3241] [flammable Solid]

67. Albb-031641

68. Hy-b1217

69. Zinc1088216

70. Tox21_112079

71. Tox21_300126

72. Bdbm50248122

73. Nsc141021

74. S4553

75. 2-bromanyl-2-nitro-propane-1,3-diol

76. Akos003606838

77. Ccg-213823

78. Cs-4699

79. Db13960

80. Bronopol 100 Microg/ml In Acetonitrile

81. Ncgc00164057-02

82. Ncgc00164057-03

83. Ncgc00253984-01

84. As-11889

85. 2-bromo-2-nitro-1,3-propanediol, 98%

86. .beta.-bromo-.beta.-nitrotrimethyleneglycol

87. Db-027831

88. B1247

89. Bronopol, Pestanal(r), Analytical Standard

90. Ft-0611399

91. 52b517

92. D01577

93. E85247

94. Ab01563195_01

95. 2-bromo-2-nitropropane-1,3-diol [inci]

96. A829125

97. Sr-01000944249

98. Q-200765

99. Q2462902

100. Sr-01000944249-1

2.4 Create Date
2005-03-25
3 Chemical and Physical Properties
Molecular Weight 199.99 g/mol
Molecular Formula C3H6BrNO4
XLogP3-0.6
Hydrogen Bond Donor Count2
Hydrogen Bond Acceptor Count4
Rotatable Bond Count2
Exact Mass198.94802 g/mol
Monoisotopic Mass198.94802 g/mol
Topological Polar Surface Area86.3 Ų
Heavy Atom Count9
Formal Charge0
Complexity107
Isotope Atom Count0
Defined Atom Stereocenter Count0
Undefined Atom Stereocenter Count0
Defined Bond Stereocenter Count0
Undefined Bond Stereocenter Count0
Covalently Bonded Unit Count1
4 Drug and Medication Information
4.1 Drug Indication

Bronopol as an active ingredient is registered as a commercial biocide and preservative in many industrial processes. Registered biocidal uses include pulp and paper mills, water cooling towers, waste water treatment, evaporative condensers, heat exchangers, food pasteurizing plants, metalworking fluids, and oilfield applications. In addition, preservative uses include household products (e.g., dishwashing liquids, laundry products), latex emulsions, polymer lattices, pigments, leather and milk samples for analysis. Bronopol is also formulated into granular domestic end-use products in the form of cat litter.


5 Pharmacology and Biochemistry
5.1 Pharmacology

At concentrations of 12.5 to 50 g/mL, bronopol mediated an inhibitory activity against various strains of Gram negative and positive bacteria _in vitro_. The bactericidal activity is reported to be greater against Gram-negative bacteria than against Gram-positive cocci. Bronopol was also demonstrated to be effective against various fungal species, but the inhibitory action is reported to be minimal compared to that of against bacterial species. The inhibitory activity of bronopol decreases with increasing pH of the media. Bronopol also elicits an anti-protozoal activity, as demonstrated with _Ichthyophthirius multifiliis_ _in vitro_ and _in vivo_. It is proposed that bronopol affects the survival of all free-living stages of _I. multifiliis_.


5.2 MeSH Pharmacological Classification

Anti-Infective Agents

Substances that prevent infectious agents or organisms from spreading or kill infectious agents in order to prevent the spread of infection. (See all compounds classified as Anti-Infective Agents.)


Anti-Infective Agents, Local

Substances used on humans and other animals that destroy harmful microorganisms or inhibit their activity. They are distinguished from DISINFECTANTS, which are used on inanimate objects. (See all compounds classified as Anti-Infective Agents, Local.)


Indicators and Reagents

Substances used for the detection, identification, analysis, etc. of chemical, biological, or pathologic processes or conditions. Indicators are substances that change in physical appearance, e.g., color, at or approaching the endpoint of a chemical titration, e.g., on the passage between acidity and alkalinity. Reagents are substances used for the detection or determination of another substance by chemical or microscopical means, especially analysis. Types of reagents are precipitants, solvents, oxidizers, reducers, fluxes, and colorimetric reagents. (From Grant and Hackh's Chemical Dictionary, 5th ed, p301, p499) (See all compounds classified as Indicators and Reagents.)


5.3 FDA Pharmacological Classification
5.3.1 Active Moiety
BRONOPOL
5.3.2 FDA UNII
6PU1E16C9W
5.3.3 Pharmacological Classes
Chemical Structure [CS] - Allergens
5.4 Absorption, Distribution and Excretion

Absorption

Bronopol was rapidly absorbed in animal studies. It may be absorbed via aerosol inhalation, dermal contact, and ingestion. In rats, approximately 40% of the topically applied dose of bronopol was absorbed through the skin within 24 hr. Following oral administration of 1 mg/kg in rats, the peak plasma concentrations of bronopol were reached up to 2 hours post-dosing.


Route of Elimination

Metabolism studies indicate that bronopol is primarily excreted in the urine. In rats, about 19% of dermally-applied bronopol was excreted in the urine, feces and expired air. Following oral administration of 1 mg/kg radiolabelled bronopol in rats, approximately 81% and 6% of the administered radioactivity was recovered in the urine and expired air, respectively, within a period of 24 hours. Following intravenous administration in rat, the recoveries in the urine and expired air were 74% and 9% of the dose, respectively.


Volume of Distribution

The highest concentrations of bronopol were detected in the excretory organs of rat such as kidney, liver, and lung. The lowest concentration was in the fat.


Clearance

No data available.


The rat metabolism data for bronopol consist of four separate studies conducted with male and female Sprague-Dawley rats. Animals were treated by gavage with (14)C bronopol (radiochemical purity: >95-100%). In the first study animals received a single dose of 10 mg/kg. The second study employed a higher dose of 50 mg/kg. Doses higher the 50 mg/kg caused respiratory problems and death. The third study's dose was 10 mg/kg (14 daily doses of nonradioactive, 100% pure, bronopol, followed by one dose of (14)C-bronopol). Urine, feces and CO2 were collected for 7 days after dosing, at which time the rats were killed and the tissues examined for radioactivity. Because, irrespective of the dose, most of the administered (14)C was excreted in urine (64-78% in 24 hours and 68-83% in 7 days), urine was used for the identification of metabolites in the fourth study. Feces, CO2 and tissues represented minor routes of excretion of (14)C. Very little (14)C was also detected in the whole blood and plasma. From the results of these four studies... /it was/ concluded that bronopol administered orally was rapidly absorbed and rapidly excreted by the rats of both sexes, with urine being the major route of excretion.

USEPA/Office of Pesticide Programs; Reregistration Eligibility Decision Document - Bronopol. Case 2770, September 1995. Available from, as of March 2, 2004: https://www.epa.gov/pesticides/reregistration/status.htm


Oral doses are rapidly absorbed and rapidly excreted, mainly in the urine /in animals/.

Tomlin CDS, ed. Bronopol (52-51-7). In: The e-Pesticide Manual, Version 2.2 (2002). Surrey UK, British Crop Protection Council.


The substance can be absorbed into the body by inhalation of its aerosol, through the skin and by ingestion.

IPCS, CEC; International Chemical Safety Card on 2-Bromo-2-nitro-1,3-propanediol. (October 1995). Available from, as of March 10, 2004: https://www.inchem.org/documents/icsc/icsc/eics0415.htm


Approximately 40% of the topically applied dose of antibacterial agent [(14)C] bronopol([(14)C]BP) was absorbed through the rat skin within 24 hr. Of the applied radioactivity, about 19% was excreted in the urine, feces and expired air. The 24 hr recoveries of (14)C in the urine and expired air were 15 and 2%, respectively, of the dose applied to the skin, and 74 and 9%, respectively, of the dose given intravenously.

PMID:7414618 Buttar HS et al; Toxicol Lett 6 (2): 101-7 (1980)


5.5 Metabolism/Metabolites

Bronopol undergoes degradation in aqueous medium to form bromonitroethanol from a retroaldol reaction with the liberation of an equimolar amount of formaldehyde. Formaldehyde is a degradation product of bronopol, which may cause sensitization. Bromonitroethanol further decomposes to formaldehyde and bromonitromethane. Bromonitroethanol may also break down to release a nitrite ion and 2-bromoethanol.


Approx. 40% of the topically applied dose of antibacterial agent [(14)C] bronopol([(14)C]BP) was absorbed through the rat skin within 24 hr. Of the applied radioactivity, about 19% was excreted in the urine, feces and expired air. The 24 hr recoveries of (14)C in the urine and expired air were 15 and 2%, respectively, of the dose applied to the skin, and 74 and 9%, respectively, of the dose given intravenously. The TLC of the urines showed three metabolites, but no unchanged [(14)C]BP in both groups. The results suggest that rat skin is quite permeable to bronopol.

Buttar HS and Downie RH. Toxicol Lett 6 (2): 101-7 (1980) 7414618


Transformation products usually differ in environmental behaviors and toxicological properties from the parent contaminants, and probably cause potential risks to the environment. Toxicity evolution of a labile preservative, bronopol, upon primary aquatic degradation processes was investigated. Bronopol rapidly hydrolyzed in natural waters, and primarily produced more stable 2-bromo-2-nitroethanol (BNE) and bromonitromethane (BNM). Light enhanced degradation of the targeted compounds with water site specific photoactivity. The bond order analysis theoretically revealed that the reversible retroaldol reactions were primary degradation routes for bronopol and BNE. Judging from toxicity assays and the relative pesticide toxicity index, these degradation products (i.e., BNE and BNM), more persistent and higher toxic than the parent, probably accumulated in natural waters and resulted in higher or prolonging adverse impacts. Therefore, these transformation products should be included into the assessment of ecological risks of non-persistent and low toxic chemicals such as the preservative bronopol.

PMID:21035931 Cui N et al; Environ Pollut 159 (2): 609-15 (2011)


The major metabolite /in animals/ has been identified as 2-nitropropane-1,3-diol.

Tomlin CDS, ed. Bronopol (52-51-7). In: The e-Pesticide Manual, Version 2.2 (2002). Surrey UK, British Crop Protection Council.


The only metabolite identified in urine was BTS 23 913 (2-nitropropane-1,3- diol or desbromo-bronopol), accounting for 45-50% of the radioactivity taken for analyses. The remaining radioactivity was not identified (one radioactive peak and radioactivity not resolved into peaks). Unchanged bronopol was not detected.

USEPA/Office of Pesticide Programs; Reregistration Eligibility Decision Document - Bronopol. Case 2770, September 1995. Available from, as of March 2, 2004: https://www.epa.gov/pesticides/reregistration/status.htm


5.6 Biological Half-Life

The half-life of bronopol in the biological systems is not reported in the literature. The half-life value reported for bronopol reflects the environment fate of the compound. When released into the air as vapours, bronopol is degraded in the atmosphere by reaction with photochemically-produced hydroxyl radicals where the half life for this reaction is approximately 11 days. The photolysis half-life is 24 hours in water but may be up to 2 days under natural sunlight.


5.7 Mechanism of Action

It is proposed that bronopol generates biocide-induced bacteriostasis followed by a growth at an inhibited rate in bacteria, via two distinct reactions between bronopol and essential thiols within the bacterial cell. Under aerobic conditions, bronopol catalyzes the oxidation of thiol groups, such as cysteine, to disulfides. This reaction is accompanied by rapid consumption of oxygen, where oxygen acts as the final oxidant. During the conversion of cysteine to cystine, radical anion intermediates such as superoxide and peroxide are formed from bronopol to exert a direct bactericidal activity. The oxidation of excess thiols alters the redox state to create anoxic conditions, leading to a second reaction involving the oxidation of intracellular thiols such as glutathione to its disulfide. The resulting effects are inhibition of enzyme function, and reduced growth rate following the bacteriostatic period. Under the anoxic conditions, the reaction between thiol and bronopol decelerates without the involvement of oxygen and the consumption of bronopol predominates. Bronopol is ultimately removed from the reaction via consumption and resumption of bacterial growth occurs.


...Under aerobic conditions, bronopol catalytically oxidizes thiol-containing materials such as cysteine, with atmospheric oxygen as the final oxidant. By-products of this reaction are active oxygen species such as superoxide and peroxide, which are directly responsible for the bactericidal activity of the compound and for the reduced growth rate after the bacteriostatic period.

PMID:3075439 Full text: https://www.ncbi.nlm.nih.gov/pmc/articles/PMC175953 Shepherd JA et al; Antimicrob Agents Chemother 32 (11): 1693-8 (1988)


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14-Feb-2021
21-Aug-2024
KGS
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Quantity (KGS) & Unit rate (USD/KGS) over time

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